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EPA Methods

Volatiles
 
Analyte Type  EPA Method Reference Common Sample  Preparation  Detector Types  Sample Matrix  Recommended Agilent Column
           
Trihalomethanes 
501
Purge and trap direct injection headspace  ELCD
ECD 
Drinking water 
124-1534
124-1334
Volatile Organic Compounds (VOCs) 502.2
8021
CLP-Volatiles   
Purge and trap direct  injection headspace   PID
ELCD  
Drinking water, waste water,
solid wastes
124-1574
124-1374
Purgeable Halogenated Organics 601 
8010
Purge and trap headspace for
screening
PID
ELCD  
Waste water,
solid wastes
124-1574
124-1374
Purgeable Aromatic Organics   503.1
602
8020 
Purge and trap headspace for screening  PID  Drinking water, waste water,
solid wastes 
124-1534
124-1334
Volatile Organic Compounds (VOCs) Using MSD  524.2 
624
8240
8260
CLP-VOCs 
Purge and trap direct injection headspace  MSD  Drinking water, waste water,
solid wastes
122-1564
122-1364
Volatile Organic Compounds (VOCs) Using 5973 MSD  524.2 624
8240 8260
CLP-VOCs 
Purge and trap direct injection headspace MSD (5973)  Drinking water,
waste water,
solid wastes
121-1524
121-1324
EDB and DBCP  504.1 8011  Microextraction with Hexane  ECD  Drinking water,
solid wastes
121-1324
124-1534
Acrylonitrile and Acrolein  603 8015 8031  Purge and trap liquid extraction sonication  FID
NPD 
Waste water,
solid wastes
124-1334
124-1534
 
Semivolatiles
 
Analyte Type  EPA Method Reference Common Sample  Preparation  Detector Types  Sample Matrix  Recommended Agilent Column
           
Semivolatile Organic Compounds   525
625
8270  
Liquid extraction sonication soxhlet  extraction SPE    MSD   Drinking water, waste water, solid wastes   
19091S-133
 Phenols   528
604
8040
8041  
Liquid extraction sonication soxhlet extractionderivatization   ECD, FID   Waste water, solid  wastes   
122-5532
122-1232
125-5532
125-6837
 Phthalate Esters   506
606
8060
8061  
Liquid extraction,  sonication soxhlet  extraction SPE      ECD
FID  
Drinking water, waste water, solid wastes   
122-5532
125-5532
125-6837
 Benzidines   605    Liquid extraction   ECD   Waste water  
122-5532
125-5532
125-6837
 Nitrosamines   607
8070  
Liquid extraction  sonication soxhlet  extraction SPE      NPD   Waste water, solid wastes    
122-5532
125-5532
Nitroaromatics and Isophorone  609
8090 
Liquid extraction  sonication soxhlet extraction SPE  ECD
FID 
Waste water, solid wastes  
19091S-133
125-5532
125-6837
Polynuclear Aromatic Hydrocarbons (PAHs)   610
8100 
Liquid extraction sonication soxhlet extraction SPE  FID  Waste water, solid wastes 
122-5532
123-5532
122-0132
Chlorinated Hydrocarbons  612
8120
8121 
Liquid extraction  sonication soxhlet extraction SPE  ECD  Waste water, solid wastes 
123-5536
19091S-113
123-103E
Chlorinated Disinfection Byproducts  551
551.1A 
Liquid extraction derivatisation  ECD  Drinking water 
122-5533
122-1033
Halogenated Acetic Acids   552
552.1 552.2 
Liquid extraction derivatisation   ECD  Drinking water 
123-3832
123-1236
 
Pesticides, Herbicides, and PCBs
 
Analyte Type  EPA Method Reference Common Sample  Preparation  Detector Types  Sample Matrix  Recommended Agilent Column
           
Organochlorine Pesticides and PCBs  552,
552.1
552.2 
Liquid extraction, derivatisation  ECD  Drinking water 
123-3832
123-1236
 
 

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