Practical GC Troubleshooting and Maintenance

2 Day Course

A logical approach to GC Troubleshooting and Maintenance is explored in this two-day course. Commonly encountered problems and best practices are examined for all major system components including gas handling, inlet system, oven, column and detector.

Examination of separation chemistry, interrogation of poor peak shape and retention problems are a fundamentally important part of the course, leading to increased awareness of troubleshooting principles. 
Practical exercises are fundamental to this course and industry standard equipment will be used to carry out a wide range of laboratory-based tasks.

  • We limit numbers to 6 per course so that each delegate gets the opportunity to ask questions and fully participate in practical exercises 
  • When delivered on-site we can design the course material to suit your specific training needs
  • Customisable written assessments are available if required


Course Overview | Download course details »

All components of the GC system and associated problems are systematically studied. The use of chromatograms as diagnostic tools is explored in depth, including baselines, peak shape and retention time inconsistencies, spurious peaks, etc.

Laboratory based sessions are included to make an all-encompassing and thorough two day course 

Who is this course for

This course is designed for those relatively new to GC, or for those users of GC systems who want to gain a deeper insight of their instruments. Ideally will follow-on from attendance to the Fundamental GC training course.

Previous knowledge

Some previous knowledge of gas chromatography and basic experience are recommended but not essential. 

What you will learn

  • Instrument problems - identifying the issues
  • Developing troubleshooting strategies
  • Column installation
  • Inlet maintenance
  • Inlet and oven parameters
  • Detector maintenance
  • Common maintenance schedule operations
  • Investigative operations

 

Course Outline

Approaches to Logical Troubleshooting

  • Logical troubleshooting
  • System overview
  • Component perspective
  • Symptomatic perspective
  • System maintenance records
  • Symptom/Causes/Diagnosis and solution

Column Installation

  • Installation and conditioning of a capillary column
  • Column length calculation
  • Run Check Out sample 
  • Time, peak area and efficiency
  • Column troubleshooting

Detector Maintenance

  • Stripping and cleaning the FID

Inlet Maintenance

  • Stripping the inlet: liner, gold seal, septum and split vent trap 
  • The gas flow path and hydraulic control
  • Pressure test inlet
  • Inlet troubleshooting

Inlet and Oven Parameters

  • The effect of split ratio on peak shape and quantitative accuracy
  • Investigating oven initial temperature
  • Inlet troubleshooting questions

Troubleshooting Strategy

  • Bringing it all together with questions and a practical challenge!