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Tosoh Bioscience EcoSEC High Temperature

The EcoSEC High Temperature GPC System from Tosoh Bioscience is a compact, all-in-one instrument developed for fast, high-resolution gel permeation chromatography at elevated temperatures – up to 220°C. Designed to meet the rigorous demands of high-temperature polymer analysis, such as for polyolefins, the system delivers reliable, reproducible results within a robust and user-friendly platform.

Building on the proven technology of the ambient EcoSEC GPC System, the High Temperature model integrates every key component into an all-in-one design. Its dual pump solvent delivery system, dual flow refractive index (RI) detector, and total system temperature control ensure precise and stable operation, even under demanding analytical conditions. The large column oven accommodates multiple columns and provides uniform heating for optimal separation performance.

The system can also be upgraded with a High Temperature Viscometer Detector, extending its analytical capabilities for comprehensive polymer characterisation.

Features

  • Dual Flow Cell RI Detector – Minimises noise and baseline drift, ensuring outstanding signal stability even at elevated temperatures
  • Constant Temperature Control – Maintains stable conditions across the degasser chamber, pump heads and solvent lines for precise and reproducible performance
  • Low Dead Volume Design – Enhances resolution and analytical accuracy while reducing solvent consumption
  • Spacious Column Oven – Accommodates up to eight columns and a switching valve, providing flexibility for complex, high-temperature analyses
  • User-Friendly Software – Offers intuitive operation and comprehensive control for efficient system management and data acquisition
  • Wide Temperature Range – Enables reliable polymer analysis at temperatures up to 220 °C, ideal for demanding high-temperature applications
  • Enhanced Safety Features – Integrated sensors provide extended safety monitoring, ensuring secure operation under high-temperature conditions
  • 24-Vial Autosampler – Equipped with temperature control up to 220 °C for automated, consistent sample handling
  • Integrated Sample Preparation System – Provides controlled heating, gentle shaking and filtration to ensure uniform sample conditioning prior to analysis

Specification

  EcoSEC High Temperature
Pump  
Flow rate 0.1 to 2.0 mL/min in 0.1 mL/min steps
Accuracy ± 2%
Precision ± 0.2%
Max pressure 15 MPA or 2,175 psi
   
Auto-injector  
Injection volume 10 to 500 µL (dependent on sample loop size)
Number of samples 24
   
Column Oven  
Temperature range 40°C to 220°C
Capacity 7.8 mm ID × 300 mm × 8 columns
   
RI Detector  
Type Bryce or dual flow type. Tungsten light source
Cell volume 10 µL
Noise 1.5 × 10-8 RI units (RIU) (ODCB: 1.0 mL/min, 145°C, response: 3 s)
Drift 3 × 10-7 RIU/h (ODCB: 1.0 mL/min, 145°C)
   
Instrument  
Dimensions Width: 100.0 cm
Depth: 50.0 cm
Height: 65.0 cm

Literature

Overview of EcoSEC ELITE and EcoSEC High Temperature GPC Systems
GPC system for demanding high temperature applications
Examples of ambient and high temperature GPC analysis for a broad range of polymers using TSKgel columns and EcoSEC GPC systems
Full range of TSKgel columns for GPC analysis
Quick reference guide for choosing a TSKgel column for polymer analysis